IB Chemistry R3.2 R3.2.1

Oxidation & Reduction

OIL RIG, rules for oxidation states, half-equations, and identifying redox agents.

Reactivity 3.2 SL & HL ⏱️ ~5 min revision
Core Definitions

Redox Principles (OIL RIG)

  • Oxidation: Loss of electrons (\(\text{OIL}\)), increase in oxidation state, or addition of oxygen.
  • Reduction: Gain of electrons (\(\text{RIG}\)), decrease in oxidation state, or loss of oxygen / gain of hydrogen.
  • Oxidising agent: Accepts electrons, oxidises another species, and is itself reduced.
  • Reducing agent: Donates electrons, reduces another species, and is itself oxidised.

RIG

Reduction Is Gain (of electrons)

Oxidising agent = accepts electrons (is itself reduced). Reducing agent = donates electrons (is itself oxidised).

Three Ways to Define Redox

Perspective Oxidation Reduction
Electrons Loss of e⁻ Gain of e⁻
Oxidation state Increase in ox. Number Decrease in ox. Number
Oxygen / Hydrogen Gain of O / Loss of H Loss of O / Gain of H

Oxidation States (Numbers)

An oxidation state is a formal charge assigned to an atom, assuming all bonds are completely ionic. It lets us track electron transfer in complex molecules.

Rules Checklist

8 Rules for Assigning Oxidation States

  1. Free uncombined elements = 0 (e.g. \(\text{O}_2, \text{P}_4, \text{Na}\)).
  2. Simple monoatomic ions = charge on ion (e.g. \(\text{Fe}^{3+} = +3, \text{Cl}^- = -1\)).
  3. Fluorine in all compounds = -1.
  4. Group 1 metals = +1; Group 2 metals = +2; Aluminium = +3.
  5. Hydrogen in compounds = +1 (except metal hydrides like \(\text{NaH}\) where it is -1).
  6. Oxygen in compounds = -2 (except peroxides like \(\text{H}_2\text{O}_2\) where -1, and in \(\text{OF}_2\) where +2).
  7. Sum of oxidation states in neutral molecule = 0.
  8. Sum of oxidation states in polyatomic ion = overall charge on ion.
Worked Example

Oxidation State of Mn in Permanganate

Problem: Find the oxidation state of Mn in \(\text{MnO}_4^-\).

\[\text{OS(Mn)} + 4(-2) = -1 \implies \text{OS(Mn)} - 8 = -1 \implies \text{OS(Mn)} = \mathbf{+7}\]

Identifying Redox Reactions

Assign oxidation states to every element on both sides. If any element's oxidation number changes, it is a redox reaction. If no elements change, it is not redox (e.g. Acid-base neutralisation).

Half-Equations

Half-equations show oxidation and reduction separately. Every redox reaction can be split into two half-equations.

Worked Example

Half-Equations: Mg + CuSO₄

Overall: \(\text{Mg}(\text{s}) + \text{CuSO}_4(\text{aq}) \rightarrow \text{MgSO}_4(\text{aq}) + \text{Cu}(\text{s})\)

  • Oxidation half-equation: \(\text{Mg}(\text{s}) \rightarrow \text{Mg}^{2+}(\text{aq}) + 2\text{e}^-\) (Mg is reducing agent)
  • Reduction half-equation: \(\text{Cu}^{2+}(\text{aq}) + 2\text{e}^- \rightarrow \text{Cu}(\text{s})\) (\(\text{Cu}^{2+}\) is oxidising agent)
Method

Balancing Complex Half-Equations (Acidic Conditions)

  1. Balance elements other than H and O.
  2. Balance oxygen atoms by adding \(\text{H}_2\text{O}\).
  3. Balance hydrogen atoms by adding \(\text{H}^+\).
  4. Balance charge by adding electrons (\(\text{e}^-\)) to the more positive side.
  5. Multiply half-equations to equate electron counts, then add and cancel spectators.
Worked Example

Balancing the Permanganate Half-Equation

1. \(\text{MnO}_4^- \rightarrow \text{Mn}^{2+}\)

2. Balance O: \(\text{MnO}_4^- \rightarrow \text{Mn}^{2+} + 4\text{H}_2\text{O}\)

3. Balance H: \(\text{MnO}_4^- + 8\text{H}^+ \rightarrow \text{Mn}^{2+} + 4\text{H}_2\text{O}\)

4. Balance charge (\(+7 \rightarrow +2\)): \(\mathbf{\text{MnO}_4^- + 8\text{H}^+ + 5\text{e}^- \rightarrow \text{Mn}^{2+} + 4\text{H}_2\text{O}}\)

Disproportionation

A reaction where a single element is simultaneously oxidised and reduced.

Example: Cl₂ + H₂O → HClO + HCl

Cl goes from 0 (in Cl₂) to both +1 (in HClO) and −1 (in HCl).

Examiner Trap

Common Redox Notation and Naming Errors

  • Charge vs Oxidation State: Charge is written \(2+\) or \(2-\); oxidation state is written \(+2\) or \(-2\) with the sign first.
  • Per-atom calculations: In \(\text{Cr}_2\text{O}_7^{2-}\), each Cr is \(+6\), not \(+12\).
  • Naming the whole agent: When asked to identify the oxidising agent, name \(\text{CuSO}_4\) or \(\text{Cu}^{2+}\), not just "Cu".
  • Stock Roman numerals: Iron(III) chloride = \(\text{FeCl}_3\); Manganese(IV) oxide = \(\text{MnO}_2\).
Key Insight

Identifying Agents in Ionic Equations

In the reaction \(2\text{Fe}^{2+} + \text{Cl}_2 \rightarrow 2\text{Fe}^{3+} + 2\text{Cl}^-\), \(\text{Fe}^{2+}\) increases from \(+2 \rightarrow +3\) (oxidised, reducing agent), and \(\text{Cl}_2\) decreases from \(0 \rightarrow -1\) (reduced, oxidising agent).

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