IB ChemistryStructure 33.23.2.9

IR Spectroscopy

Identifying functional groups from characteristic absorption peaks.

Structure 3.2 HL Extension ⏱️ ~5 min revision

Key Absorptions (From Data Booklet)

Bond Wavenumber / cm⁻¹ Appearance Indicates
O-H (alcohol) 3200-3550 Broad Alcohol
O-H (acid) 2500-3300 Very broad Carboxylic acid
N-H 3300-3500 Medium, often 2 peaks Amine / amide
C=O 1700-1750 Strong, sharp Aldehyde, ketone, acid, ester
C-O 1000-1300 Strong Alcohol, ester, ether
C=C 1620-1680 Medium Alkene
IR Regions

Diagnostic Region vs Fingerprint Region (< 1400 cm⁻¹)

Below ~\(1400\text{ cm}^{-1}\) is the fingerprint region: a complex pattern of bending and stretching vibrations unique to each molecule. It is used for computer database comparison rather than individual peak assignment.

Functional group diagnosis focuses on the functional group region (\(1500\text{--}4000\text{ cm}^{-1}\)).

Exam Tip

Carboxylic Acid Pattern: Broad O-H + Sharp C=O

A very broad absorption band at \(2500\text{--}3300\text{ cm}^{-1}\) (O–H acid) plus a sharp strong absorption at \(1700\text{--}1750\text{ cm}^{-1}\) (C=O carbonyl) is the unmistakable diagnostic signature of a carboxylic acid.

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