IB Chemistry R3.4 R3.4.1
R3.4.1 HL

Free Radical Substitution

Why Are Alkanes Generally Unreactive?

Alkanes contain only strong, non-polar C−C and C−H bonds. There are no lone pairs, no regions of high/low electron density, and no functional groups. So they are not attacked by nucleophiles or electrophiles under normal conditions.

Exception: Under UV light (or high temperature), halogen molecules undergo homolytic fission to form free radicals, which are reactive enough to attack C−H bonds.

Bond Fission

Homolytic Fission

Bond breaks equally. One electron to each atom

Produces free radicals (species with unpaired electrons, shown with •)

Cl−Cl → Cl• + Cl•

Shown with fish-hook (single-barbed) curly arrows

Heterolytic Fission

Bond breaks unequally. Both electrons to one atom

Produces ions (cation + anion)

H−Br → H⁺ + Br⁻

Shown with full (double-barbed) curly arrows

The Free Radical Substitution Mechanism

Alkanes react with halogens under UV light via a free radical mechanism. This has three stages:

Chemistry diagram 1. Initiation Cl₂ → 2Cl (UV light breaks Cl−Cl = homolytic fission) Each atom gets one electron → free radicals 2. Propagation (chain reaction) Cl• + CH₄ → CH₃• + HCl (radical attacks methane) CH₃• + Cl₂ → CH₃Cl + Cl• (radical regenerated) One radical consumed, one produced → chain continues 3. Termination Cl• + Cl• → Cl₂ CH₃• + Cl• → CH₃Cl CH₃• + CH₃• → C₂H₆ Two radicals combine → chain ends

Key Features of Each Stage

  • Initiation: UV light provides the energy for homolytic fission of Cl₂. This is the rate-determining step. No reaction without UV light
  • Propagation: A self-sustaining chain reaction. Each step consumes one radical and produces another. There are always exactly two propagation steps
  • Termination: Any two radicals combine. These are minority reactions. The chain typically propagates hundreds of times before termination

Limitations of Free Radical Substitution

⚠️ Why It Gives a Mixture of Products

  • Poly-substitution: Once CH₃Cl is formed, it has C−H bonds that can react further: CH₃Cl → CH₂Cl₂ → CHCl₃ → CCl₄
  • Unexpected termination products: e.g. CH₃• + CH₃• → C₂H₆ (ethane, not expected from a methane + chlorine reaction)
  • Low selectivity: Radicals are so reactive they attack almost any C−H bond, even in longer chains (producing multiple positional isomers)

This makes free radical substitution of limited synthetic value. Mixtures are hard to separate and purify.

Reactivity Order of Halogens

F₂ > Cl₂ > Br₂ > I₂. Fluorine is too reactive (explosive), iodine is too unreactive (endothermic). Chlorine and bromine are most commonly used.

Think About It

Why does free radical substitution typically give a mixture of products?

Further substitution can occur: CH₃Cl → CH₂Cl₂ → CHCl₃ → CCl₄. Also, termination can produce unexpected products like ethane (C₂H₆) when two methyl radicals combine.

⚠️ Common Exam Mistakes

  • Using full curly arrows instead of fish-hook arrows. Radicals involve single electron movement
  • Forgetting to state UV light as the condition for initiation
  • Writing only one propagation step. You must write both
  • Confusing homolytic fission (→ radicals) with heterolytic fission (→ ions)
← Back to R3.4R3.4.2 Nucleophilic Sub. →